Spark Plasma Sintering of Ultra-High Temperature Tantalum/Hafnium Carbides Composite

Flash (Ultra-Rapid) Spark-Plasma Sintering of Silicon Carbide

A new ultra-rapid process of flash spark plasma sintering is developed. The idea of flash spark plasma sintering (or flash hot pressing - FHP) stems from the conducted theoretical analysis of the role of thermal runaway phenomena for material processing by flash sintering. The major purpose of the present study is to theoretically analyze the thermal runaway nature of flash sintering and to exp...

Spark Plasma Sintering of Negative Temperature Coefficient Thermistor Ceramics

Comparison of Reactive and Non-Reactive Spark Plasma Sintering Routes for the Fabrication of Monolithic and Composite Ultra High Temperature Ceramics (UHTC) Materials

A wider utilization of ultra high temperature ceramics (UHTC) materials strongly depends on the availability of efficient techniques for their fabrication as dense bodies. Based on recent results reported in the literature, it is possible to state that Spark Plasma Sintering (SPS) technology offers a useful contribution in this direction. Along these lines, the use of two different SPS-based pr...

Effect of SiC nanoparticles addition on mechanical properties and wear resistance of cemented carbides fabricated by spark plasma sintering

WC-10Co cemented carbides containing 1 to 4 wt% SiC nanoparticles were prepared by spark plasma sintering. The effects of SiC content on microstructure, mechanical properties and wear resistance of the sintered materials were studied. Microstructural studies showed that SiC addition resulted in WC grain coarsening. In addition, the hardness decreased with increasing SiC content. However, the fr...

Fabrication of Nanostructured Cu matrix Nanocomposites by High Energy Mechanical Milling and Spark Plasma Sintering

Spark plasma sintering (SPS) is a sintering process that is capable of sintering hard worked powders in short times. This technique was used to fabricate bulk Cu and Cu-SiC nanocomposites. Pure Cu and mixed powders of Cu including 4 vol% of SiC nanoparticles were mechanically alloyed for 25 h and sintered at 750˚C under vacuum condition by SPS method. Microstructures of the materials were chara...

Phase and Microstructural Correlation of Spark Plasma Sintered HfB2-ZrB2 Based Ultra-High Temperature Ceramic Composites

Abstract: The refractory diborides (HfB2 and ZrB2) are considered as promising ultra-high temperature ceramic (UHTCs) where low damage tolerance limits their application for the thermal protection system in re-entry vehicles. In this regard, SiC and CNT have been synergistically added as the sintering aids and toughening agents in the spark plasma sintered (SPS) HfB2-ZrB2 system. Herein, a nove...